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5 h, the reaction mixture was diluted with EtOAc, and quenched with 2 M aq NaOH. The organic layer was separated, and the aqueous layer was extracted with EtOAc twice. The combined organic layers were washed with brine, dried with MgSO4, and filtered. 03 mmol, 71 %) as a yellowish solid. 7 mmol, 56 %) was recovered as a yellowish solid. mp 140–141 °C [lit. 2767. Methyl 3-(2,4-dihydroxy-3,6-dimethylbenoyl)-4-hydroxy-6-methoxy-2,5-dimet hylbenzoate (11). 50 g, 50 wt%) at room temperature, and the flask was purged with hydrogen 7 times.
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