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17. 18. 19. ; Natusch, D. F. , Anal. Chem. 1982, J54, 26Α. Hercules, D. ; Day, R. ; Dang, T. ; Li, C. , Anal. Chem. 1982, 54, 280A. , Med. Prog. Technol. 1979, £, 109-21. , unpublished studies, University of Pittsburgh, 1982. Schiller, C ; Krupke, K. , Z. Anal. Chem. » 30*· Jordan, K. D · , unpublished studies, University of Pittsburgh, 1982. ; Destefano, A. ; Sanders, R. , Org. Mass Spectrom. 1980, JLjs 348. Sanders, R. ; Destefano, A. , Org. Mass Spectrom. 1980, JJ^, 348. Bowie, J. , Org. Mass Spectrom.
Strong chelating agents such as bipyridine, o-phenanthroline and porphyrins generally show this kind of behavior. This is not universal, because decomposition of the ions occurs and in some cases the fully coordinated M L n + (L = ligand) is not observed, but loss of 1 or 2 ligands is responsible for the major peak. At the other end of the scale, we have studied coordination compounds of cobalt containing amine and polyamine-acid ligands and have found that extensive decomposition is observed for these compounds.
Destefano, A. ; Sanders, R. , Org. Mass Spectrom. 1980, JLjs 348. Sanders, R. ; Destefano, A. , Org. Mass Spectrom. 1980, JJ^, 348. Bowie, J. , Org. Mass Spectrom. 1972, £ , 429. Gardella, J. ; Hercules, D. ; Heinen, H. , Spectrosc. Letters, 1980, 21» 347. Gardella, J. ; Hercules, D. , Z. Anal. Chem. 1981, 308, 297. 41 2 PYROLYSIS AND DESORPTION MASS SPECTROMETRY. Robert J . Cotter, Department of Pharmacology, The Johns Hopkins U n i v e r s i t y , Baltimore, Maryland 21205 (USA) Field desorption (FD), secondary ion mass spectro- metry (SIMS), plasma desorption (PDMS), laser desorp t i o n (LD), and f a s t atom bombardment (FAB) techniques have greatly increased the c a p a b i l i t y of mass spectrometry f o r analyzing l a r g e , n o n - v o l a t i l e molecules.