By Irmgard Bartenieff
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Mol. Struct. 4 (1969) 221. 3(15) Mn−C(eq)≡O ) Assumed. ) The C≡O bond is bent towards the H atom. : Inorg. Chem. 33 (1994) 1217. 1606(10) ) Uncertainties are slightly larger than those of the original data. : J. Mol. Spectrosc. 62 (1976) 175. 132 a) θ0 C(ax)−Re−C(eq) deg 96(1) ) Assumed. : J. Chem. Phys. 99 (1993) 6465. 340(1) 3,5-Bis(trifluoromethyl)pyrazole θ a) C=C–CF3 N=C–CF3 C–C–F C1 deg b) 129(2) 119(1) 111(1) The nozzle temperature was 77 °C. a ) Unidentified, possibly ra and θa. ) Estimated standard errors.
Mol. Struct. 130 (1985) 255. : Z. Naturforsch. 30a (1975) 1765. 535 b) Pentacarbonylgermylmanganese(I) deg a) θa 110 b) H−Ge−H 97(2) C(ax)−Mn−C(eq) 180 b) Mn−C(eq)≡O Free rotation and C3v symmetry of the GeH3 group was assumed. The nozzle temperature was 60 °C. a ) Estimated standard errors including a systematic error. ) Assumed. : J. Organomet. Chem. 85 (1975) 225. 521 b) Pentacarbonylgermylrhenium(I) θa Re−Ge−H C(ax)−Re−C(eq) Re−C(eq)≡O deg a) 111 b) 97(2) 178(2) c) Free rotation and C3v symmetry of the GeH3 group was assumed.
Fitted parameter. : J. Mol. Spectrosc. 141 (1990) 325. 5 c) The orientation of the ONO plane with respect to the ring plane was not stated in the original paper. The nozzle temperature was 150 °C. ) Unidentified, possibly ra and θa. ) Three times the estimated standard errors. c ) Derived from the final radial distribution refinement. Uncertainties are rather large. : J. Mol. Struct. 96 (1982) 151. 036 N N N NH The observed spectrum was assigned to the N(9)H tautomer (see figure). : Chem. Phys.