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Ion Association in Proton Transfer Reactions. Use of ESR for by J. R. Jones, A. A. Westenberg, K. R. Jennings and R. B.

25 February 2017 adminGeneral Reference

By J. R. Jones, A. A. Westenberg, K. R. Jennings and R. B. Cundall (Auth.)

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Extra resources for Ion Association in Proton Transfer Reactions. Use of ESR for the Quantitative Determination of Gas Phase Atom and Radical Concentrations

Sample text

H & 0*893 v. , line A is Mj = 1/2 -> 3/2, Mj = 3/2 and line B is AT, = 1/2 -> 3/2, Mj = 1/2. The corresponding transitions for Br 79 0 (51 % abundance) lie about 16 G above their Br 81 0 counterparts, so that the two isotopie species appear as doublets. 64 The three sets of ΔΜ, = 1 lines intermingle but the three lowest field transitions are line A: Mj = 1/2 -> 3/2, ΜΣ = 5/2; line B: M3 = 1/2 -> 3/2, M, = 3/2; line C: M, - 1/2 -> 3/2, Ml = 1/2, respectively. The whole 16-line pattern spreads over about 1500 G centered at H ^ 0-893 v.

Table 11 labels the transitions. The C1370 spectrum mingles with that of C1350, corresponding lines being within a few gauss of each other, with C1370 spread out slightly less. BrO(2Z73/2) This spectrum is basically similar to ClO and was actually analyzed64 from the results obtained using electric field (Stark) modulation65 rather than the usual magnetic field (Zeeman) modulation. This had certain practical advantages—mainly the elimination of interfering lines due to 0 2 , which has no permanent dipole moment and therefore no Starkmodulated spectrum.

The level for which the total angular momentum quantum number / = 3/2. 5, 49 Each line is actually a doublet due to the two components — <-►+. These are not resolved at pressures above a few tenths of a torr, 42 A. A. WESTENBERG although the splitting (~ IG) has been observed6' 49 at lower pressures. 18 The value49 of gj = 0-7772, so the spectrum is centered at a field given nearly by H ^ 0-9193 J>. There are three groups of three lines, the groups being about 45 G apart and the lines in each group about 27 G apart.

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