By G. Schudt-Weitz, I. Strell (auth.), K.-H. Hellwege, A. M. Hellwege (eds.)
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11. Diffractometer measurement; anisotropic refinement. 048. 19. Deep red cubic crystals (from methanol). Film data. 090. See also LB 16-48-2. Pale blue platelets elongated along c, (010) developed (from methyl ethyl ketone). Diffractometer measurement; anisotropic relinement; hydrogen positions determined. 077. ’ N-CH, ‘W -4 2COCIL [ I I -Cl Cl-cu ‘V Cl (J-6 n E X 8 No. (Subst. ) Author 3224 SL Space group Cdl dimensions eerp[s/cd Additional remarks. Further informations. [Al z R. T [“I Formula wt.
21 y&)0) Colourless prismatic needles (from methanol/acetone). Diffractometer measurement; anisotropic refinement ; hydrogen positions determined; abso lute configuration determined. 047. [20350-15-61 3176 SL C,6H,,0,Pt, Di-p-allyl-bis(2,4-pentanedionato)diplatinum P&/c 3177 C,,H,,Co wz n-Cyclooctenyl-n-(l,S-cyclooctadiene)3178 cobalt; (1,5-Cyclooctadiene-n-2-cycioSL octen- 1-yI)cobalt ]11082-48-7. 11072-42-7. 80(2) ... 3) ... 146. Brilliant black plates (from n-hexane); sensitive to air and RT.
094. CH, 3196 3197 (ReO;& 3202 S-&H5 I H,C, H,C’ CjH I 2 CHz i,C’ CH, I S-&H5 3200 3199 HJ\ CHx I H& CH, co \ / co H,C~Sn\~u/Sn\~u/Co OC’ I ‘Sn’ Co / \ W ‘3 CH, I ‘Sn’ Co 1 ‘CH, H,C I e W N-Be-N CHs -2+ 3201 CHJ 3 y ‘0 3203 H& \ /W’s n - Substance (Subst. ) Author T No. iUlt1 3204 SL Ccl1 dimensions P4,/mmm y k/cm- 1 Formula wt. -No. 0 Additional remarks. Further informations. R. Footnotes. Crystals not stable in the open air (from mercury cyanide in tetrahydrofuran). sensitive to X-rays. Film data; anisotropic rctincmcnt; hydrogen positions determined.